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Molecular Chemistry book from C.H.I.P.S.

Analytical Methods in Supramolecular Chemistry
edited by Christoph A. Schalley

Analytical Methods in Supramolecular Chemistry is a definitive survey of useful modern analytical methods for understanding supramolecular chemistry, from NMR to single-molecule spectroscopy to extraction methods.

Contents

Introduction

  • Some Historical Remarks on Supramolecular Chemistry
  • The Noncovalent Bond: A Brief Overview
  • Basic Concepts in Supramolecular Chemistry
  • Conclusions: Diverse Methods for a Diverse Research Area

Determination of Binding Constants

  • Theoretical Principles
  • A Practical Course of Binding Constant Determination by UV/vis Spectroscopy
  • Practical Course of Action for NMR Spectroscopic Binding Constant Determination

Isothermal Titration Calorimetry in Supramolecular Chemistry

  • The Thermodynamic Platform
  • Acquiring Calorimetric Data
  • Extending the Applicability
  • Perspectives

Extraction Methods

  • The Extraction Technique
  • The Technical Process
  • The Extraction Equilibrium
  • Principles of Supramolecular Extraction
  • Examples of Supramolecular Extraction
  • Conclusions and Future Perspectives

Mass Spectrometry and Gas Phase Chemistry of Supramolecules

  • Instrumentation
  • Particuliarities and Limitations of Mass Spectrometry
  • Beyond Analytical Characterization: Tandem MS Experiments for the Examination of the Gas-phase Chemistry of Supramolecules
  • Selected Examples

Diffusion NMR in Supramolecular Chemistry

  • Concepts of Molecular Diffusion
  • Measuring Diffusion with NMR
  • Applications of Diffusion NMR in Supramolecular Chemistry: Selected Examples
  • Advantages and Limitations of Diffusion NMR
  • Diffusion NMR and Chemical Exchange
  • Summary and Outlook

Photophysics and Photochemistry of Supramolecular Systems

  • Spectrophotometry and Spectrofluorometry
  • Time-resolved Fluorescence Techniques
  • Fluorescence Anisotropy
  • Transient Absorption Spectroscopy

Circular Dichroism Spectroscopy

  • Basic Considerations
  • Measurement Techniques (Methodology of CD Measurement)
  • Processing of Circular Dichroism Spectra
  • Theory
  • Examples of Vibrational Circular Dichroism Applications

Crystallography and Crystal Engineering

  • Crystallography
  • Crystal Engineering

Scanning Probe Microscopy

  • Introduction: What is the Strength of Scanning Probe Techniques?
  • How do Scanning Probe Microscopes Work?
  • Which Molecules can be Studied?
  • What Results have been Obtained in the Field of Supramolecular Chemistry?

The Characterization of Synthetic Ion Channels and Pores

  • Methods
  • Characteristics
  • Structural Studies

Theoretical Methods for Supramolecular Chemistry

  • A Survey of Theoretical Methods
  • Standard Classification of Intermolecular Interactions
  • Qualitative Understanding and Decomposition Schemes
  • General Mechanism for a Static, Step-wise View on Host–Guest Recognition

Index

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Analytical Methods in Supramolecular Chemistry
edited by Christoph A.Schalley
2007 • 484 pages • $214.00 + shipping
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