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Industrial Chemistry Book from C.H.I.P.S.

Instrumental Methods in Metal Ion Speciation
by Imran Ali

Instrumental Methods in Metal Ion Speciation introduces the principles of metal ion speciation and discuss important analytical techniques such as gas and liquid chromatography, capillary electrophoresis, and both electrochemical and radiochemical methods used to determine concentration and composition.

Features:

  • Describes occurrence, distribution, and toxicities of all metal ion species
  • Details gas, ion, and liquid chromatography for metal ion speciation, including reverse HPLC, ion-pair, size exclusion, chiral, and supercritical fluid methods
  • Covers various capillary electrophoresis, spectroscopic, electrochemical, and radiochemical methods for speciation
  • Contains detailed sample preparation techniques and appropriate metal ion speciation from environmental and biological samples
  • Explains the role of metal ion speciation in risk assessment and legislation

Contents

Introduction

  • Importance of the Environment
  • Environmental Pollutants
  • Metal Ions Speciation
  • Metal Ion Speciation and the Environment
  • Methods Of Metal Ion Speciation
  • Detection in Chromatography and Capillary Electrophoresis

Mtal Ion Species: Sources and Distribution

  • Sources of Contamination
  • Distribution of Metal Ions
  • Mechanisms of Metal Ions Contamination

Metal Ion Species: Toxicities, Biotransformation, and Biodegradation

  • Modes of Bioactivity and Toxicities of Metal Ions
  • Toxicities of Metal Ions
  • Biotransformation of Metal Ions
  • Biodegradation of Metal Ions
  • Essentiality versus Toxicity of Metal Ions

Sample Preparation

  • Sampling
  • Preservation
  • Filtration
  • Digestion/Homogenization
  • Extraction
  • Membrane Methods in Sample Preparation
  • Enzymatic Hydrolysis
  • Other Extraction Methods
  • Cleanup
  • Preconcentration

Speciation of Metal Ions by Gas Chromatography

  • Applications
  • Optimization of Metal Ion Speciation
  • Derivatization of Metal Ions
  • Mechanisms of Metal Ions Speciation
  • Errors and Problems in Metal Ions Speciation

Speciation of Metal Ions by Reversed-Phase High-Performance Liquid Chromatography

  • Applications
  • Optimization of Metal Ion Speciation
  • Derivatization of Metal Ions
  • Mechanisms of Metal Ions Speciation

Speciation of Metal Ions by Ion Chromatography

  • Applications
  • Optimization of Metal Ion Speciation
  • Mechanisms of Metal Ions Speciation

Speciation of Metal Ions by Ion-Pair, Micellar Electrokinetic, Size Exclusion, Chiral, Capillary Electro-, and Supercritical Fluid Chromatographic Methods

  • Ion-Pair Chromatography
  • Micellar Electrokinetic Chromatography
  • Size Exclusion Chromatography
  • Chiral Chromatography
  • Capillary Electrochromatography
  • Supercritical Fluid Chromatography
  • Mechanisms
  • LC versus GC

Speciation of Metal Ions by Capillary Electrohoresis

  • Application of Capillary Electrophoresis for the Speciation of Metal Ions
  • Optimization of the Speciation
  • Validation of the Methods
  • Effect of Interfering Ions
  • Mechanisms of Metal Ion Speciation
  • Capillary Electrophoresis versus Chromatography

Speciation of Metal Ions by Spectroscopic Methods

  • UV-Visible Spectroscopy
  • Atomic Absorption Spectroscopy
  • Inductively Coupled Plasma Spectrometry
  • Mass Spectrometry
  • X-Ray Spectroscopy
  • Miscellaneous Spectroscopic Methods

Speciation of Metal Ions by Electrochemical and Radiochemical Methods

  • Electrochemical Methods
  • Radiochemical Methods
  • Miscellaneous Methods

Perspectives and Legislation of Metal Ion Speciation

  • The Future of Speciation
  • Risk Assessment and Legislation
  • Metal Ion Speciation and Legislation
  • International Scenario of Legislation

Index

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Instrumental Methods in Metal Ion Speciation
by Imran Ali
2006 376 pages $168.95 + shipping
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